(北京有色金属研究总院 有色金属材料制备与加工国家重点实验室,北京100088)
摘 要: 为研究钛合金的热压缩变形过程中流变应力、显微组织等随变形条件的变化,对自行研制的Ti-3.0Al- 3.7Cr-2.0Fe低成本钛合金在Gleeble−1500D 热模拟实验机上进行高温压缩变形实验。对d 8 mm×12 mm的试样进行等温压缩变形实验,研究该合金在变形量为30%、50%和70%(对应真应变为1.2)、变形温度为800~950 ℃、应变速率为0.01~10 s−1条件下的变形行为、流变应力的变化规律以及变形条件对显微组织的影响。结果表明:该合金流变应力受变形温度和应变速率影响显著,流变峰值应力随变形温度的升高和应变速率的降低而降低。采用Arrhenius双曲正弦模型确定该合金在本实验条件下的变形激活能Q=214.22 kJ/mol和应力指数n=3.81,并根据得到的参数建立相应的热变形本构关系为 =6.91×108[sinh(0.011σ)]3.81exp[−214 220/(RT)]。通过显微组织观察发现,在950 ℃、变形速率≥0.1 s−1时,发生再结晶现象,且随着变形速率的增加,再结晶现象越明显。
关键字: 钛合金;Ti-3.0Al-3.7Cr-2.0Fe;热压缩;本构关系;显微组织
(State Key Laboratory of Nonferrous Metals and Processes,
General Research Institute for Nonferrous Metals, Beijing 100088, China)
Abstract:In order to study the change of flow stress and microstructures with deformation condition, the hot compressive deformation behavior of self-made Ti-3.0Al-3.7Cr-2.0Fe low cost titanium alloy was investigated by Gleeble−1500D thermal simulator. The test conditions were set as follow, the strain rate ranges from 0.01 s−1 to 10 s−1, the temperature ranges from 800 ℃ to 950 ℃ and the deformation is almost 70% which equal to the true strain of 1.2. The test results indicate that the peak flow stress decreases with the decreasing test temperature and increasing the strain rate. The constitutive relationship of Ti-3.0Al-3.7Cr-2.0Fe alloy is obtained on the base of Arrhenius equations. When the strain rates are higher than 0.1 s−1, the dynamic recrystallization occurs in the alloy, and the higher the strain rates are, the more the evident recrystallization is.
Key words: titanium alloy; Ti-3.0Al-3.7Cr-2.0Fe; hot compressive; constitutive relationship; microstructure