Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

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中国有色金属学报

ZHONGGUO YOUSEJINSHU XUEBAO

第29卷    第4期    总第241期    2019年4月

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文章编号:1004-0609(2019)-04-0684-09
5083铝合金中θ-Al45(Mn,Cr)7相的孪晶现象
肖晓玲1,刘宏伟2,陈文龙1,詹 浩1,孙红英1

(1. 广东省工业分析检测中心,广州 510650;
2. Australian Centre for Microscopy & Microanalysis, The University of Sydney, Sydney 2006 Australia
)

摘 要: 应用高分辨透射电镜观察了5083铝合金轧制退火组织中弥散相的形态和微观结构。结果表明:呈球状或不规则形状、尺寸约200~300 nm的弥散相为θ-Al45(Mn,Cr)7相,属单斜结构,晶胞大小a=2.5196 nm,b=0.7574 nm,c=1.0949 nm,β=128.72°。另外,还发现该相颗粒内部易产生孪晶、孪晶畴和复合孪晶,伴有二次孪晶(或微孪晶)和反相畴界等晶体缺陷,孪晶面分别为 或 ,共轭面为 或 。同时从晶体学角度解释了该相孪晶和复合孪晶等缺陷的生成机制。

 

关键字: 5083铝合金;透射电镜;θ-Al45(Mn,Cr)7相;孪晶

Twinning of θ-Al45(Mn,Cr)7 phase in 5083 aluminum alloy
XIAO Xiao-ling1, LIU Hong-wei2, CHEN Wen-long1, ZHAN Hao1, SUN Hong-ying1

1. Guangdong Industrial Analysis and Testing Center, Guangzhou 510650, China;
2. Australian Centre for Microscopy & Microanalysis, The University of Sydney, Sydney 2006, Australia

Abstract:The morphology and microstructure of dispersoids in 5083 alloy with H116 temper condition were investigated using JEOL 2100F transmission electron microscope equipped with EDS and STEM. The results show that the discrete spherical-like or irregular-shaped θ-Al45(Mn,Cr)7 phase which has monoclinic structure with a unit cell of a=2.5196 nm, b=0.7574 nm, c=1.0949 nm, β=128.72° is observed in 5083 alloy. One type of twin is shown to be a or twin with the or plane serving as the twinning plane, and another type of orientation twin is seen to be a domain with the plane serving as the coherent plane. The boundaries of both domain and twin are found to be coincident with the twinning plane. In addition composite-twins are also observed in θ-Al45(Mn,Cr)7 particles. Possible formation mechanisms of the twins are discussed based on a crystallographic consideration.

 

Key words: 5083 aluminium alloy; TEM; θ-Al45(Mn,Cr)7 phase; twin

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

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