中国有色金属学报(英文版)
Transactions of Nonferrous Metals Society of China
Vol. 28 No. 6 June 2018 |
(1. School of Metallurgical and Ecological Engineering, University of Science and Technology Beijing, Beijing 100083, China;
2. Key Lab of Electromagnetic Processing of Materials, Ministry of Education, Northeastern University, Shenyang 110819, China)
Abstract:The grain refinement of the as-cast AZ31 alloys by limestone particles was investigated by grain refining tests and microstructure observations. The results show that the limestone particles have a good grain refining potency, which is deeply related to the addition level of limestone and melting temperature. The optimal addition level and melting temperature are 2.0% (mass fraction) and 720 °C, respectively. The average grain size of AZ31 alloy is reduced from (556±60) to (236±22) μm. The sound grain refining by raw limestone particles has a good anti-fading capacity without any significant grain coarsening in a 40 min holding time. The concerned grain refining mechanism should be attributed to the inoculated Al-C and Al-C/Al-Mn-(Fe) nuclei. Ultrasonic treatment can enhance the grain refining efficiency of limestone particles through cavitation-enhanced nucleation mechanism.
Key words: AZ31 magnesium alloy; grain refinement; limestone ore; microstructure; ultrasonic treatment