(1. Department of Engineering, Faculty of Materials Science and Engineering,
Imam Hossein University, Tehran 15816-18711, Iran;
2. Young Researchers and Elite Club, Science and Research Branch, Islamic Azad University, Tehran 14515775, Iran;
3. Department of Material Engineering, South Tehran Branch, Islamic Azad University, Tehran 1459853849, Iran)
摘 要: 采用扩散连接方法在压力范围10~35 MPa、温度430~450 °C、时间60 min，真空13.3 mPa条件下连接Al 7075和 Mg AZ31合金。采用扫描电子显微镜、X射线能谱和X射线衍射分析合金的显微组织演变、相分析和元素分布。结果表明:25 MPa为最佳的压力条件，在此条件下接头发生最小的塑性变形；在界面过渡区可观察到含不同金属间化合物如Al12Mg17, Al3Mg2 和 α(Al)的固溶体反应层；随着温度的升高，反应层的厚度增大，更多的铝原子扩散进入镁合金，且界面朝着铝合金移动；在温度440 °C、压力25 MPa下得到最大的结合强度38 MPa。断口形貌研究表明，脆性断裂来自于Al3Mg2相。
关键字: Al 7075合金；Mg AZ31合金；扩散连接；金属间化合物；界面过渡区；显微组织；力学性能
（1. Department of Engineering, Faculty of Materials Science and Engineering,
Imam Hossein University, Tehran 15816-18711, Iran;
2. Young Researchers and Elite Club, Science and Research Branch, Islamic Azad University, Tehran 14515775, Iran;
3. Department of Material Engineering, South Tehran Branch, Islamic Azad University, Tehran 1459853849, Iran）
Abstract:Al 7075 and Mg AZ31 alloys were joined by diffusion bonding method. Joining process was performed in pressure range of 10-35 MPa at temperatures of 430-450 °C for 60 min under a vacuum of 13.3 MPa. The microstructure evaluation, phase analysis and distribution of elements at the interface were done using scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS) and X-ray diffraction (XRD). The pressure of 25 MPa was determined as the optimum pressure in which the minimum amount of plastic deformation takes place at the joint. Different reaction layers containing intermetallic compounds, such as Al12Mg17, Al3Mg2 and α(Al) solid solution, were observed, in interfacial transition zone (ITZ). Thickness of layers was increased with increasing the operating temperature. According to the results, diffusion of aluminum atoms into magnesium alloy was more and the interface movement towards the Al alloy was observed. The maximum bond strength of 38 MPa was achieved at the temperature of 440 °C and pressure of 25 MPa. Fractography studies indicated that the brittle fracture originated from Al3Mg2 phase.
Key words: Al 7075 alloy; Mg AZ31 alloy; diffusion bonding; intermetallic compounds; interfacial transition zone; microstructure; mechanical properties
