Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

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中国有色金属学报

ZHONGGUO YOUSEJINSHU XUEBAO

第25卷    第10期    总第199期    2015年10月

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文章编号:1004-0609(2015)10-2745-07
热等静压制备CF/Al复合材料的微观结构及性能
喻思1,郎利辉1,姚松2,王刚1,黄西娜1,续秋玉1

(1. 北京航空航天大学机械工程及自动化学院,北京 100191;
2. 中国工程物理研究院化工材料研究所,绵阳621900
)

摘 要: 采用热等静压(HIP)工艺制备连续碳纤维(CF)增强Al基复合材料。利用扫描电镜、粒度仪和X射线衍射仪表征2A12铝合金粉末形貌、粒度分布和相组成;利用光学显微镜、扫描电镜和能谱仪观察复合材料的显微组织、断口形貌和界面扩散反应特征,并对其主要力学性能进行测试。结果表明:粉末形貌呈球形,粒度主要分布在150~180μm;复合材料致密,界面连接紧密无孔洞缺陷;与基体铝合金材料相比,复合材料的拉伸强度和断后伸长率分别提高5%和54%,断裂方式为脆性断裂;Al基体裂纹起源于粉末颗粒界面,CF/Al界面断口呈现CF拔出和断裂失效形式;CF/Al界面发生元素扩散,界面反应生成Al4C3金属间化合物。

 

关键字: CF/Al复合材料;热等静压;失效形式;界面反应

Microstructure and properties of CF/Al composite manufactured by hot isostatic pressing
YU Si1, LANG Li-hui1, YAO Song2, WANG Gang1, HUANG Xi-na1, XU Qiu-yu1

1. School of Mechanical Engineering and Automation, Beihang University, Beijing 100191, China;
2. Institute of Chemical Materials, China Academy of Engineering Physics, Mianyang 621900, China

Abstract:Aluminum matrix composite reinforced with continuous carbon fiber (CF) was manufactured by hot isostatic pressing (HIP). The morphology, grain size distribution and phase of the powders were investigated by scanning electron microscope (SEM), particle analyzer and X-ray diffraction (XRD). The microstructure, fracture surface morphologies and CF/Al interface reaction characteristic were observed by optical microscope (OM), scanning electron microscope (SEM) and energy dispersive spectrometer (EDS). The mechanical properties of the composites were also tested. The results indicate that, the powders are nearly spherical, the particle size is mainly 150-180μm; the compositesare compact and the interface bonding is tight without porosity defect; compared with the aluminum matrix alloy, the tensile strength and elongation of the composites increase by above 5% and 54%, respectively, and the fracture mechanism is brittle fracture; the fracture of the Al matrix is along the powder interface, carbon fibers are pulled out and fractured in the CF/Al interface zone; the interface of the CF/Al appears element diffusion, and the interfacial reaction product is Al4C3 intermetallic compound.

 

Key words: CF/Al composite; hot isostatic pressing; failure mode; interfacial reaction

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

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