中国有色金属学报(英文版)
Transactions of Nonferrous Metals Society of China
Vol. 24 No. 1 July 2014 |
(1. School of Nano & Advace Material Engineering, Changwon National University,Changwon 641-773, Korea;
2. Department of Mechanical Engineering, Changwon National University,Changwon 641-773, Korea)
Abstract:Coatings on Mg alloys were prepared using NaOH + Na2SiO3 as basic electrolyte containing electrolyte of Na2SiF6 or NaF. EPP treatment was carried out on AZ31 Mg alloys matrix under a hybrid voltage of AC of 200 V combined with DC of 260 V for 30 min. Structural and morphological analyses of ceramic coatings were analyzed by XRD and SEM. Wear and hardness of coatings were measured by pin-on disk test and Vickers hardness test. The coatings formed in Na2SiF6 and NaF electrolytes were mainly composed of MgO and Mg2SiO4. The measured micro-hardness of coating formed in Na2SiF6 electrolyte was found to be over HV 1100, while, coating formed in NaF electrolyte possessed micro-hardness of HV ~900. These results show that the mechanical properties of AZ31B Mg alloys can be enhanced by the proper selection of electrolyte agent.
Key words: AZ31B Mg alloy; surface treatment; electrolytic plasma processing