Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

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中国有色金属学报

ZHONGGUO YOUSEJINSHU XUEBAO

第9卷    第4期    总第33期    1999年12月

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文章编号:1004-0609(1999)04-0769-05
AlN陶瓷自蔓延高温合成
郑永挺     王华彬    韩杰才    杜善义     赫晓东

(哈尔滨工业大学 复合材料研究所,  哈尔滨 150001)

摘 要:

 

关键字: AlN陶瓷;自蔓延高温合成;致密化

Self-propagating high-temperature synthesis of AlN ceramic
Zheng Yongting, Wang Huabin, Han Jiecai, Du Shanyi, He Xiaodong

Center for Composite Materials, Harbin Institute of Technology, Harbin 150001, P. R. China

Abstract:Full conversion AlN ceramics with approximately 80% relative density were fabricated by self-propagating high-temperature synthesis(SHS) of Al particles in high pressure nitrogen. The effects of initial factors such as the content of diluent, nitrogen pressure and the porosity of compacts on the conversion and relative density of products were discussed in detail. Full conversion and relative density of AlN ceramics were synthesized by addition of appropriate diluents. At the lower level of the diluent in the sample, nitrogen gas is difficult to infiltrate due to aggregation of molten Al, Al cannot completely converse into AlN.As the content of the diluents is up to 60%, self-propagating high-temperature synthesis reaction cannot be self-sustained.With increasing of the pressure of nitrogen, the conversion of product increases and the relative density of the ceramics is improved. The low or high relative density of the sample is not benefit to improve the relative density of the ceramics.

 

Key words: AlN ceramics; self-propagating high-temperature synthesis; densification

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

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