(1. 中国科学院过程工程研究所 多相复杂系统国家重点实验室,北京 100190;
2. 中国科学院 研究生院,北京 100049;
3. 北京科技大学 循环与生态冶金教育部重点实验室,北京 100083)
摘 要:
关键字: 镍箔;超重力场;重力系数;电沉积;结构;性能
(1. State Key Laboratory of Mutiphase Complex System, Institute of Process Engineering, Chinese Academy of Sciences, Beijing 100190, China;
2. Graduate University of Chinese Academy of Sciences, Beijing 100049, China;
3. Laboratory of Ecological and Recycle Metallurgy, University of Science and Technology Beijing, Beijing 100083, China)
Abstract:In a high gravity field vertical to electrode surface, the effects of high gravity on the microstructure and properties of Ni film deposited electrochemically were investigated. With atomic force microscopy (AFM) and X-Ray diffraction. The results reveal that the surface structure of nickel film deposited under high gravity condition was more uniform and smoother compared with that in normal gravity condition; under G = 354, the roughness decreased sharply from 20.9 nm to 4.9 nm, and crystal grains diminished with the increasing of gravity coefficient. Furthermore, its crystal structure transforms from tropism to non-tropism with gravity coefficient. The hardness and tensile stress of nickel film are raised markedly to HV898 and 944 MPa when the gravity coefficient was up to 354 g, higher than those in normal gravity condition by HV604 and 646 MPa, respectively.
Key words: nickel film; high gravity field; gravity coefficient; electro-deposition; structure; property