Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

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中国有色金属学报

ZHONGGUO YOUSEJINSHU XUEBAO

第18卷    第7期    总第112期    2008年7月

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文章编号:1004-0609(2008)07-1261-07
MB8镁合金阴极电沉积Ni-SiC纳米复合镀层微观结构及性能
李雪松1, 2,吴 化1,杨 友1,江中浩2

(1. 长春工业大学 材料科学与工程学院,长春 130012;
2. 吉林大学 汽车材料教育部重点实验室,长春 130025
)

摘 要:

采用以硫酸镍为主盐的电沉积技术,在MB8形变镁合金表面制备纳米复合镀层。利用扫描电镜和透射电镜观察复合镀层的显微形貌和微观结构,利用X射线衍射仪和能谱仪对复合镀层进行物相分析,利用显微硬度计测定镀层显微硬度,利用快速磨损试验机测试复合镀层的耐磨性能,利用电化学测试仪测定复合镀层在3.5%NaCl(质量分数)溶液中的极化曲线。结果表明:在MB8形变镁合金表面可以获得结晶均匀、结构致密的纳米复合镀层,该复合镀层的显微硬度最高达HV 682,其耐磨性能超过硬铬镀层,且具有较好的耐蚀性能,自腐蚀电位较镁合金基体提高677 mV。

 

关键字: MB8镁合金;电沉积;纳米复合镀层;纳米SiC

Microstructure and properties of cathode electrodeposited Ni-SiC nano composite coatings on MB8 magnesium alloy
LI Xue-song1, 2, WU Hua1, YANG You1, JIANG Zhong-hao2

1. College of Materials Science and Engineering, Changchun University of Technology, Changchun 130012, China;
2. Key Laboratory of Automobile Materials, Ministry of Education, Jilin University, Changchun 130025, China

Abstract:Nano composite coatings were prepared on MB8 wrought magnesium alloy by electrodeposition with sulfate nickel as main salt. The microstructure of the composite coatings were observed with scanning electron microscopy and transmission electron microscopy, its phase compositions were analyzed with X-ray diffractometry, its microhardness was determined with microhardness meter, its abrasive resistance was tested by rapid abrasive test, and its polarization curve in 3.5% (mass fraction) sodium chloride solution was determined by electrochemical tester. The results show that nano composite coatings with uniform crystalline, dense structure and better corrosion resistance can be obtained on MB8 wrought magnesium alloy and its maximum microhardness reaches HV 682. Moreover, the abrasive resistance of the composite coatings is superior to that of the hard chromium coating, the corrosion potential is increased by 677 mV compared with base Mg alloy.

 

Key words: MB8 magnesium alloy; electrodeposition; nano composite coating; nano-SiC

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

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