Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

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中国有色金属学报(英文版)

Transactions of Nonferrous Metals Society of China

Vol. 22    No. 8    August 2012

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Effect of mechanical attrition on microstructure and property of electroplated Ni coating
BAN Chao-lei1,2, SHAO Xin1,2, MA Jie1,2, CHEN Hui1,2

1. School of Materials Science and Technology, Liaocheng University, Liaocheng 252059, China;
2. Liaocheng Research Institute of Nonferrous Metals, Liaocheng 252059, China

Abstract:Ni coating was deposited on carbon steel by a mechanical attrition enhanced electroplating (MAEE) process. During the electroplating, the mechanical attrition(MA) was introduced by impact of glass balls on the sample surface with a special vibrating frequency. The surface and cross-sectional images of Ni coating were observed with SEM. The microstructure and crystallinity of coating were examined with TEM and XRD. The electrochemical performance of coating was measured with polarization curves and electrochemical impedance spectroscopy (EIS) and its mechanical behaviours, such as tensile strength and hardness, were studied. The results show that the MA has significant effects on the microstructure and property of the electroplated Ni coating. By MA, the coating becomes smooth, compact, thin and has refined grains and is free of cracks and pores. Consequently, the adhesion, tensile strength, hardness and corrosion resistance of coating are improved significantly.

 

Key words: electroplating; mechanical attrition; Ni coating; corrosion resistance

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

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