中国有色金属学报(英文版)
Transactions of Nonferrous Metals Society of China
Vol. 13 Special 1 May 2003 |
(1. National Key Laboratory of Advanced Welding Production Technology,
Harbin Institute of Technology,Harbin 150001, China;
2. Key Lab of Liquid Structure and Heredity of Materials,
Shandong University, Jinan 250061, China)
Abstract:The sound joints of Fe3Al intermetallics and Q235 low carbon steel dissimilar materials were made by vacuum diffusion bonding process at 1050-1100℃,9.8MPa held for 1h. Microstructure and composition characteristics at the interface of Fe3Al/Q235 were studied by means of scanning electron microscopy(SEM), X-ray diffractometry(XRD), electron probe micro-analysis(EPMA) and transmission electron microscopy(TEM). The results indicate there exits FeAl phases and α-Fe (Al) solid solution near the Fe3Al/Q235 interface. Aluminum content decreases from 28% to 1.5% and corresponding phase changes from Fe3Al with DO3 type body-centered cubic (bcc) structure to α-Fe (Al) solid solution, and both structures have an orientation relationship of crystal (11-0)α-Fe(Al)‖(011)Fe3Al and [001]α-Fe(Al)‖[100]Fe3Al. Based on this, a formation mechanism of the interface structure was elucidated.
Key words: Fe3Al intermetallics; vacuum diffusion bonding; microstructure; element transition