Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

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中国有色金属学报

ZHONGGUO YOUSEJINSHU XUEBAO

第12卷    第6期    总第51期    2002年12月

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文章编号:1004-0609(2002)06-1104-05
硅元素对钽丝再结晶行为的影响
张新明, 袁 韧, 周卓平

(中南大学 材料科学与工程学院, 长沙 410083)

摘 要: 采用显微硬度测量、 取向分布函数(ODF)分析及显微组织观察, 研究了在不同退火温度以及掺硅与未掺硅条件下钽丝的再结晶行为。 研究发现: 在1360℃退火时掺硅对钽丝的再结晶有阻碍作用, 晶粒变细, 丝织构主要由{110}〈001〉组成; 当退火温度升高至1500℃时,  {120}〈001〉再结晶织构消失, 在未掺硅钽丝中发现了新的{441}〈110〉织构组分, 与初次再结晶织构组分{120}〈001〉之间存在一个近似于84°〈110〉的转动关系, 此时, 掺入硅元素反而促进了再结晶的发展, 晶粒变得粗大且不均匀。 这种现象可以用硅化物的形成与溶解来解释。

 

关键字: 钽丝; 掺硅; 再结晶; 织构

Effect of silicon on recrystallization behavior oftantalum wires during annealing
ZHANG Xin-ming, YUAN Ren, ZHOU Zhuo-ping

School of Materials Science and Engineering,
Central South University, Changsha 410083, China

Abstract:The recrystallization textures of the tantalum wires with silicon additives(0.01%) after annealed at different temperatures were investigated by ODF, and the recrystallization mechanism was studied by microstructures and hardness measurement. It is found that the recrystallization temperature increases with silicon additives after annealed below 1360℃ and the main texture component consists of {110}〈001〉, but at 1500℃, the exaggerated growth occurs. The size of recrystallized grains grows larger and a new component {441}〈110〉 having an 84°〈110〉 orientation relationship to the primary texture {120}〈001〉 is found. The reason for the exaggeration may be the dissolution of dislocation-silicon atom pairs.

 

Key words: tantalum wires; silicon additives; recrystallization; texture

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

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