Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

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中国有色金属学报(英文版)

Transactions of Nonferrous Metals Society of China

Vol. 18    No. 4    August 2008

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Preparation of nano-Ag/TiO2 thin-film
PENG Bing(彭 兵), WANG Jia(王 佳), CHAI Li-yuan(柴立元),MAO Ai-li(毛爱丽), WANG Yun-yan(王云燕)

School of Metallurgical Science and Engineering, Central South University, Changsha 410083, China

Abstract:Steady TiO2 water-sol was prepared by peptization and the effects of pH value, temperature, concentration of colloid and peptizator on sol were investigated. Laser grain analyzer was used to verify nano-particles in the sol. The photocatalytic degradation ratio and antibacterial property of nano-Ag/TiO2 thin-film on ceramics were used as the main index in addition to XRD analysis. The effect of film layers, embedding Ag+, annealing temperature and time on the degradation ratio and antibacterial property was studied. The temperature 30−80 ℃, pH 1.2−2.0, concentrations of 0.05−0.3 mol/L sol and 5% HNO3 would be the optimal parameters for the TiO2 water-sol preparation. The nano-Ag/TiO2 film of three layers with 3% AgNO3 embedded and treated at 350 ℃ for 2 h exhibits good performance. The elementary research on the kinetics of degradation shows that the reactions are on the first order kinetics equation.

 

Key words: nano-Ag/TiO2; water-sol; film; thermal treatment

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

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